🔴 Legionella in Water

Microbiology PN-EN ISO 11731

Detection and quantitative determination of Legionella bacteria in water by culture method on BCYE/GVPC medium with heat or acid treatment. The only method recognized by Sanepid.

Overview

Legionella is a genus of Gram-negative rods, of which the most dangerous to humans is Legionella pneumophila — the causative agent of legionellosis (Legionnaires' disease), severe pneumonia with 5–30% mortality. Legionella bacteria naturally inhabit aquatic environment, but pose a health risk when they multiply in artificial water systems: hot water installations, cooling towers, fountains, jacuzzis, humidifiers and air conditioners.

Infection occurs by inhalation — through inhaling water aerosol containing bacteria. Legionella is not transmitted from person to person. Optimal multiplication temperature: 25–45°C, with maximum at 35–37°C. Below 20°C bacteria do not grow, above 60°C they die.

The culture method according to PN-EN ISO 11731:2017 is the only method recognized by the State Sanitary Inspectorate in Poland. It includes membrane filtration or direct plating, preliminary sample treatment (heat 50°C/30 min or acid pH 2.2/5 min) to eliminate accompanying flora, culture on GVPC medium (selective) and BCYE (non-selective) at 36±1°C in moist atmosphere for 7–10 days.

Testing is required by the Regulation of the Minister of Health on water quality in internal installations (≤100 cfu/100 mL — no action, >100 — cleaning and disinfection, >1000 — immediate corrective actions). Waiting period for results: 9–15 days, which is the main disadvantage of the culture method.

Method principle

The water sample is concentrated by membrane filtration (0.2 µm) or centrifugation. The concentrate is subjected to treatment eliminating accompanying flora: heat treatment (50±1°C/30 min) or acid treatment (HCl/KCl buffer pH 2.2 for 5 min). The sample is plated on GVPC medium (BCYE agar with supplements: glycine, polymyxin B, vancomycin, cycloheximide — inhibiting bacteria and fungi) and on BCYE medium without supplements (control). Incubation: 36±1°C in moist atmosphere (>80% RH) for 7–10 days. Legionella colonies: grayish, glassy, with "cut-glass" structure. Confirmation: no growth on BCYE without L-cysteine (Legionella requires L-cysteine for growth).

Applications

Key parameters

ParameterValue
Resultcfu/100 mL (colony forming units)
Permissible value≤100 cfu/100 mL (no action), >1000 — alarm
Incubation temperature36 ± 1°C
Incubation time7–10 days (reading after 3, 5, 7 and 10 days)
AtmosphereAerobic, humidity >80% RH
Waiting time for result9–15 days (with treatment and confirmation)

Standard

Standard number
PN-EN ISO 11731:2017
Title (PL)
Jakość wody — Oznaczanie ilościowe Legionella
Title (EN)
Water quality — Enumeration of Legionella

Step-by-step procedure

1. Sample collection

Collect min. 1 L water. DO NOT rinse sampling point (no flushing). Add sodium thiosulfate (if chlorinated water). Transport at 5–20°C, analysis within 24 h.

⏱ Time: 10 min

2. Membrane filtration — concentration

Filter 1 L sample through 0.2 µm filter (polycarbonate). Aseptically cut membrane, place in sterile container with 10 mL of reserved sample. Vortex vigorously 2 min.

⏱ Time: 15 min

3. Heat treatment

Divide concentrated sample into 2 portions. Heat one in water bath 50±1°C for 30 min (elimination of heat-sensitive flora). Leave the other without treatment.

⏱ Time: 35 min • 🌡 Temperature: 50 ± 1°C

4. Acid treatment (alternative)

Instead of heat treatment: add HCl/KCl buffer (pH 2.2) in 1:1 ratio. Contact 5 min. Then neutralize with KOH buffer.

⏱ Time: 10 min

5. Plating on media

Plate 0.1 mL sample (treated and untreated) on GVPC and BCYE plates. Spread with glass spatula. Plate in duplicate.

⏱ Time: 10 min

6. Incubation

Incubate plates at 36±1°C in moist atmosphere (>80% RH). Use tightly sealed bags or incubator with water tray. DO NOT invert plates.

⏱ Time: 7–10 days • 🌡 Temperature: 36 ± 1°C

7. Reading — day 3 and 5

Check plates under stereomicroscope. If accompanying flora overgrows GVPC plates — perform additional plating with another treatment.

⏱ Time: 15 min

8. Reading — day 7 and 10

Count colonies with typical morphology: grayish, glassy, shiny, with "cut-glass" structure. Diameter 1–3 mm. Mark suspect colonies.

⏱ Time: 20 min

9. Confirmation — subculture

Transfer suspect colonies to BCYE with L-cysteine and BCYE without L-cysteine. Incubate 36°C/48 h. Growth on BCYE+cysteine and no growth on BCYE−cysteine = Legionella spp.

⏱ Time: 48 h • 🌡 Temperature: 36°C

10. Serogroup identification

Test confirmed Legionella colonies with latex test (agglutination) to identify L. pneumophila sg 1 (most commonly pathogenic) and sg 2–14.

⏱ Time: 15 min

11. Result calculation

Result = (number of confirmed colonies × dilution factor) / sample volume. Report in cfu/100 mL or cfu/L.

12. Quality control

Positive control: L. pneumophila ATCC 33152. Negative control: sterile water. Check incubator humidity and media sterility.

⏱ Time: 15 min

Required equipment and apparatus

EquipmentExampleIndicative price
Membrane filtration system (0.2 µm)Sartorius Combisart, Merck EZ-Fit with 0.2 µm filters3,000–12,000 PLN
Incubator with humidity controlBinder KBF 115, Memmert HPP110 with water tray8,000–25,000 PLN
Thermostatic water bathMemmert WNB 14, Julabo CORIO C-B5 (50°C for heat treatment)5,000–15,000 PLN
Laboratory vortexIKA Vortex 3, Scientific Industries Vortex-Genie 21,500–4,000 PLN
AutoclaveTuttnauer ELV 254020,000–45,000 PLN
Class II laminar flow hoodEsco Airstream Class II, Telstar Bio II Advance20,000–50,000 PLN
StereomicroscopeZeiss Stemi 305, Olympus SZ615,000–15,000 PLN

Reagents, media and consumables

ReagentCASDetails
BCYE Agar (Buffered Charcoal Yeast Extract)Base medium with L-cysteine, ferric pyrophosphate, activated carbon, yeast extract, ACES buffer. Manufacturers: Oxoid, Merck, bioMérieux
GVPC Agar (selective supplement)BCYE + glycine + polymyxin B + vancomycin + cycloheximide. Inhibits accompanying flora
BCYE without L-cysteineControl medium — Legionella does not grow without L-cysteine. For confirmation
L-Cysteine hydrochloride52-89-1BCYE growth supplement, concentration 0.4 g/L. Legionella requires L-cysteine
Acid buffer HCl/KCl pH 2.2For acid treatment of sample — elimination of accompanying flora. Contact 5 min
Membrane filters 0.2 µm (polycarbonate)Polycarbonate (PC), 47 mm, black or white. For filtration of Legionella samples
Latex test reagentsLatex agglutination test for identification of L. pneumophila serogroups (sg 1–14). Oxoid DR0800

Health and safety (OHS)

🔍 Find a laboratory performing this test